Как выбрать гостиницу для кошек
14 декабря, 2021
In a typical synthesis, reported by our group [45], a total amount of 1.00 g of P123 was placed in a flask and 47.80 mL of distilled H2O, 3.42 mL concentrated HCl and 2.45 mL 1-butanol were added. The solution was stirred for 1.5 h at room temperature and subsequently 1.86 mL of E-BTSE was added to the mixture. Next, the mixture was vigorously stirred at 35 °C. After 4 h, the temperature was raised to 90 °C and aged for 16 h. Afterwards, the mixture was left to cool down, and the white solid was filtered and washed with acetone and distilled water. Finally, P123 was removed via Soxhlet extraction with acetone for 5 h. The white solid, denoted as EP, was dried at 120 °C under vacuum (~0.1 Pa).